6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

Base Information

Chemical Name:6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine
CAS No.:206354-38-3
Molecular Formula:C₂₈H₂₆ClN₂O₃
Molecular Weight:473.979
Hs Code.:

Synonyms:6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

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Chemical Property of 6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

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Technology Process of 6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

There total 3 articles about 6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 76893-27-1
(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-yl)methyl methanesulfonate

: 206354-37-2
2-(tert-Butyl-dimethyl-silanyloxy)-6-chloro-9-phenoxy-acridine

: 206354-38-3
6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.25h;
DOI:10.1016/S0960-894X(98)00089-4

Reference yield:

: 191214-93-4
2-hydroxy-6,9-dichloroacridine

: 206354-38-3
6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / imidazole / dimethylformamide / 24 h / Ambient temperature

2: 80 percent / 1 h / 80 °C

3: 34 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(98)00089-4

Reference yield:

: 206354-36-1
2-(tert-Butyl-dimethyl-silanyloxy)-6,9-dichloro-acridine

: 206354-38-3
6-chloro-2-[(1-oxyl-2,2,5,5-tetramethyl-pyrrolin-3-yl)methyloxy]-9-phenoxy-acridine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 1 h / 80 °C

2: 34 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0960-894X(98)00089-4