N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1431302-67-8
Molecular Formula:C₂₂H₃₆N₂O₃SSi
Molecular Weight:436.691
Hs Code.:

Synonyms:N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

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Chemical Property of N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

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Technology Process of N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

There total 4 articles about N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 288264-99-3,7086-80-8
(2R,5S)-2-hydroxy-2-methyl-5-(prop-1-en-2-yl)cyclohexanone

: 1431302-67-8
N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

2: methanol / 5 h / 20 °C

With 2,6-dimethylpyridine; In methanol; dichloromethane;
DOI:10.1021/ol400754e

Reference yield:

: 203719-53-3
(-)-limonene oxide

: 1431302-67-8
N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium phosphate / aq. phosphate buffer / 32 h / 20 °C / pH 3.1

2: 2-iodoxybenzoic acid / ethyl acetate / 16 h / Reflux

3: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

4: methanol / 5 h / 20 °C

With 2,6-dimethylpyridine; potassium phosphate; 2-iodoxybenzoic acid; In methanol; aq. phosphate buffer; dichloromethane; ethyl acetate;
DOI:10.1021/ol400754e

Reference yield:

: 59121-82-3
(1R,2R,4S)-1-methyl-4-(prop-1-en-2-yl)cyclohexane-1,2-diol

: 1431302-67-8
N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 2-iodoxybenzoic acid / ethyl acetate / 16 h / Reflux

2: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

3: methanol / 5 h / 20 °C

With 2,6-dimethylpyridine; 2-iodoxybenzoic acid; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ol400754e