ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

Base Information

Chemical Name:ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate
CAS No.:1338473-78-1
Molecular Formula:C₂₂H₁₇Cl₃F₄N₂O₄
Molecular Weight:555.741
Hs Code.:

Synonyms:ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

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Chemical Property of ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

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Technology Process of ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

There total 1 articles about ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338473-77-0
1-{2-fluoro-5-[5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl]phenyl}methanamine hydrochloride

: 36239-09-5
ethyl chlorocarbonylacetate

: 1338473-78-1
ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;

Reference yield: 97.0%

: 1338473-78-1
ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

: 1338473-79-2
3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoic acid

Guidance literature:: ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate; With water; sodium hydroxide; In ethanol; at 20 ℃; for 2h;

With hydrogenchloride; In water; ethyl acetate;

Reference yield:

: 1338473-78-1
ethyl 3-(2-fluoro-5-(5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)benzylamino)-3-oxopropanoate

: 1338473-58-7
N-Cyclopropylmethyl-N'-{2-fluoro-5-[5-(3,4,5-trichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-benzyl}-malonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / ethanol / 2 h / 20 °C

2: triethylamine; HATU / N,N-dimethyl-formamide / 72 h / 20 °C

With water; triethylamine; HATU; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;