2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

Base Information

Chemical Name:2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine
CAS No.:1536349-25-3
Molecular Formula:C₂₉H₂₆O₄S₂
Molecular Weight:502.655
Hs Code.:

Synonyms:2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

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Chemical Property of 2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

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Technology Process of 2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

There total 1 articles about 2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1536348-94-3
6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine-2,10-diol

: 74-88-4
methyl iodide

: 1536349-25-3
2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

Guidance literature:: 6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine-2,10-diol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

methyl iodide; With 18-crown-6 ether; at 0 - 20 ℃; for 12.25h; Inert atmosphere;
DOI:10.1021/jo402522y

Reference yield: 71.0%

: 1536349-25-3
2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

: 1455435-75-2
4,4′-bis(phenylsulfanyl)-2,2′-dihydroxy-5,5′-dimethoxybiphenyl

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; for 12h;
DOI:10.1021/jo402522y

Reference yield: 21.0%

: 1536349-25-3
2,10-dimethoxy-6,6-dimethyl-3,9-bis(phenylthio)dibenzo[d,f][1,3]dioxepine

: C₂₉H₂₈O₄S₂

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; for 3.5h; Reflux; Inert atmosphere;
DOI:10.1002/chem.201903436