3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane

Base Information

• Chemical Name: 3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane
• CAS No.: 104759-28-6
• Molecular Formula: C₃₃H₅₂O
• Molecular Weight: 464.775
• Mol file: 104759-28-6.mol

Synonyms:3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane

Chemical Property of 3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane

There total 1 articles about 3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dihydrocholesterone (566-88-1) + phenylmagnesium bromide → 3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane (104759-28-6) + 3α-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3β-phenyl-5α-gonane (104759-97-9)

Guidance literature:

With tetrahydrofuran;

DOI:10.1021/ja01509a044

Reference yield: 90.0%

3β-hydroxy-10.13-dimethyl-17β-((R)-1.5-dimethyl-hexyl)-3α-phenyl-5α-gonane (104759-28-6) → 3-phenylcholest-2-ene (72457-81-9)

Guidance literature:

silica gel; toluene-4-sulfonic acid; In benzene; for 0.5h; Ambient temperature;

DOI:10.1055/s-1985-31463

upstream raw materials:

dihydrocholesterone

Downstream raw materials:

3-phenylcholest-2-ene