12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

Base Information

Chemical Name:12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan
CAS No.:112999-98-1
Molecular Formula:C₂₆H₄₄O₄
Molecular Weight:420.633
Hs Code.:

Synonyms:12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

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Chemical Property of 12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

Chemical Property:

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Technology Process of 12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

There total 4 articles about 12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 55359-65-4
1-methoxymethoxy-2-methylbenzene

: 112999-97-0,88517-92-4
2-[(12-bromododecyl)oxy]tetrahydro-2H-pyran

: 112999-98-1
12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane;

Reference yield:

: 3344-77-2
12-bromododecanol

: 112999-98-1
12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridinium-p-toluenesulfonate / CH₂Cl₂ / 12 h / Ambient temperature

2: 67 percent / 1.5 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 5675-51-4
1,12-dodecandiol

: 112999-98-1
12-<2'-(Methoxymethoxy)-3'-methylphenyl>-2-<(RS)-2-tetrahydropyranyloxy>dodecan

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 48 percent aqueous HBr / 12 h / 80 - 90 °C / darkness

2: 85 percent / pyridinium-p-toluenesulfonate / CH₂Cl₂ / 12 h / Ambient temperature

3: 67 percent / 1.5 M BuLi, N,N,N',N'-tetramethylethylenediamine / hexane; tetrahydrofuran

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen bromide; pyridinium p-toluenesulfonate; In tetrahydrofuran; hexane; dichloromethane;