allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside
CAS No.:628281-00-5
Molecular Formula:C₄₁H₄₇N₃O₁₃
Molecular Weight:789.836
Hs Code.:

Synonyms:allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Chemical Property of allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Technology Process of allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

There total 17 articles about allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 628280-91-1
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: methyl 2,4-di-O-acetyl-3-O-benzyl-α,β-L-idopyranyluronate trichloroacetimidate

: 628281-00-5
allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1.5h;
DOI:10.1016/j.tetlet.2004.03.046

Reference yield: 81.0%

: 87327-03-5
methyl (2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyl bromide)uronate

: 628280-91-1
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 628281-00-5
allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃;
DOI:10.1002/ejoc.200300254

Reference yield: 70.0%

: 75-36-5
acetyl chloride

: 628281-02-7
allyl (methyl 3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: Acetic acid (1R,3R,4R,7S,8S)-3-((2R,3S,4R,5R,6S)-6-allyloxy-5-azido-4-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-8-benzyloxy-6-oxo-2,5-dioxa-bicyclo[2.2.2]oct-7-yl ester

: (2R,3S,4R,5R,6R)-3-Acetoxy-6-((2R,3S,4R,5R,6S)-6-allyloxy-5-azido-4-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy)-4-benzyloxy-5-hydroxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 628281-04-9
allyl (methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 628281-00-5
allyl (methyl 2,4-di-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: allyl (methyl 3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-O-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside; With di(n-butyl)tin oxide; In benzene; at 90 ℃; for 0.5h;

acetyl chloride; With triethylamine; at 20 ℃; for 1h; pH=8;
DOI:10.1002/ejoc.200300254