Technology Process of Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-hydroxy-, (1S-exo)- (9CI)
There total 2 articles about Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-hydroxy-, (1S-exo)- (9CI) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; potassium permanganate;
In
hexane; water;
1.) 55 deg C, 4 h, 2.) r.t., 20 h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / H2 / 10percent Pd/C / ethyl acetate / 2.5 h
2: 70 percent / KMnO4, 6N KOH / hexane; H2O / 1.) 55 deg C, 4 h, 2.) r.t., 20 h
With
potassium hydroxide; potassium permanganate; hydrogen;
palladium on activated charcoal;
In
hexane; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating
2: 97 percent / Na2HPO4*7H2O, NaIO4 / H2O / 0.5 h / 20 °C
With
sodium periodate; disodium hydrogenphosphate; lithium aluminium tetrahydride;
In
tetrahydrofuran; water;