hexaphenylcarbodiphosphorane

Base Information

• Chemical Name: hexaphenylcarbodiphosphorane
• CAS No.: 103559-83-7
• Molecular Formula: C₃₇H₃₀P₂
• Molecular Weight: 536.593

Synonyms:hexaphenylcarbodiphosphorane

Chemical Property of hexaphenylcarbodiphosphorane

Chemical Property:

Purity/Quality:

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Technology Process of hexaphenylcarbodiphosphorane

There total 8 articles about hexaphenylcarbodiphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methylenebis(triphenylphosphonium) dibromide (14529-09-0,87978-12-9) → hexaphenylcarbodiphosphorane (103559-83-7)

Guidance literature:

With potassium hexamethylsilazane; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere; Glovebox;

DOI:10.1039/c6dt03453e

Reference yield: 50.0%

C37H30ClP2*Cl(1-) → hexaphenylcarbodiphosphorane (103559-83-7)

Guidance literature:

With Hexamethylphosphorous triamide; In benzene; for 24h; Inert atmosphere;

DOI:10.1002/adsc.201100287

Reference yield: 50.0%

tetrachloromethane (56-23-5) + triphenylphosphine (603-35-0) → hexaphenylcarbodiphosphorane (103559-83-7)

Guidance literature:

In benzene; 1.) 60 deg C, 2h, 2.) room temperature, 1 d;

upstream raw materials:

methylenebis(triphenylphosphonium) dibromide

C₃₇H₃₀P₂S

tetrachloromethane

triphenylphosphine

Downstream raw materials:

1:1-Addukt aus Hexaphenylcarbodiphosphoran u. p-Tolylisothiocyanat (Inneres Salz)

1:1-Addukt aus Hexaphenylcarbodiphosphoran u. Phenylisothiocyanat (Inneres Salz)

1:1-Addukt aus Hexaphenylcarbodiphosphoran u. p-Nitrophenylisothiocyanat (Inneres Salz)

O₂CC(PPh₃)2

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