3-methylbutyl 3-phenylpropyl sulfide

Base Information

• Chemical Name: 3-methylbutyl 3-phenylpropyl sulfide
• CAS No.: 410080-31-8
• Molecular Formula: C₁₄H₂₂S
• Molecular Weight: 222.395
• Mol file: 410080-31-8.mol

Synonyms:3-methylbutyl 3-phenylpropyl sulfide

Chemical Property of 3-methylbutyl 3-phenylpropyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-methylbutyl 3-phenylpropyl sulfide

There total 1 articles about 3-methylbutyl 3-phenylpropyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-Bromo-3-phenylpropane (637-59-2) + 3-methylbutanethiol (541-31-1) → 3-methylbutyl 3-phenylpropyl sulfide (410080-31-8)

Guidance literature:

3-methylbutanethiol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

1-Bromo-3-phenylpropane; In tetrahydrofuran; at 20 ℃; for 15h; Further stages.;

DOI:10.1021/jo016200q

Reference yield:

bromocyane (506-68-3) + 3-methylbutyl 3-phenylpropyl sulfide (410080-31-8) → 1-Bromo-3-phenylpropane (637-59-2) + (3-thiocyanatopropyl)benzene (79528-83-9)

Guidance literature:

In methanol; at 20 ℃;

DOI:10.1021/jo016200q

Reference yield:

3-methylbutyl 3-phenylpropyl sulfide (410080-31-8) → (3-thiocyanatopropyl)benzene (79528-83-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: methanol / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: 68 percent / tetrahydrofuran / 15 h / 20 °C

3.1: methanol / 0.75 h / 20 °C

With sodium hydride; In tetrahydrofuran; methanol; 1.1: von Braun reaction / 3.1: von Braun reaction;

DOI:10.1021/jo016200q

upstream raw materials:

1-Bromo-3-phenylpropane

3-methylbutanethiol

Downstream raw materials:

1-Bromo-3-phenylpropane

(3-thiocyanatopropyl)benzene

3-phenylpropyl 2-(trimethylsilyl)ethyl sulfide