2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

Base Information

Chemical Name:2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one
CAS No.:1448591-89-6
Molecular Formula:C₃₁H₂₈O₂
Molecular Weight:432.562
Hs Code.:

Synonyms:2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

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Chemical Property of 2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

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Technology Process of 2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

There total 5 articles about 2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 6261-32-1
(E)-2-benzylidene-1-tetralone

: 39110-81-1
(2-methylnaphthalen-1-yl)propan-1-one

: 1448591-89-6
2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

Guidance literature:: (2-methylnaphthalen-1-yl)propan-1-one; With tetra-(n-butyl)ammonium iodide; potassium hydroxide; In water; dimethyl sulfoxide; for 0.75h; Inert atmosphere; Schlenk technique;

(E)-2-benzylidene-1-tetralone; In water; dimethyl sulfoxide; for 4.5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201300557

Reference yield:

: 100-52-7
benzaldehyde

: 1448591-89-6
2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 24 h / Inert atmosphere; Schlenk technique

2.1: tetra-(n-butyl)ammonium iodide; potassium hydroxide / water; dimethyl sulfoxide / 0.75 h / Inert atmosphere; Schlenk technique

2.2: 4.5 h / Inert atmosphere; Schlenk technique

With tetra-(n-butyl)ammonium iodide; potassium hydroxide; In ethanol; water; dimethyl sulfoxide;
DOI:10.1002/chem.201300557

Reference yield:

: 1448591-97-6
1-(2-methylnaphthalen-1-yl)propan-1-ol

: 1448591-89-6
2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: chromium(VI) oxide; sulfuric acid / water; acetone / 1.5 h / Inert atmosphere; Schlenk technique; Cooling with ice

2.1: tetra-(n-butyl)ammonium iodide; potassium hydroxide / water; dimethyl sulfoxide / 0.75 h / Inert atmosphere; Schlenk technique

2.2: 4.5 h / Inert atmosphere; Schlenk technique

With chromium(VI) oxide; sulfuric acid; tetra-(n-butyl)ammonium iodide; potassium hydroxide; In water; dimethyl sulfoxide; acetone;
DOI:10.1002/chem.201300557