Technology Process of 2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one
There total 5 articles about 2-[2-methyl-3-(2-methylnaphthalen-1-yl)-3-oxo-1-phenylpropyl]-3,4-dihydronaphthalen-1-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(2-methylnaphthalen-1-yl)propan-1-one;
With
tetra-(n-butyl)ammonium iodide; potassium hydroxide;
In
water; dimethyl sulfoxide;
for 0.75h;
Inert atmosphere;
Schlenk technique;
(E)-2-benzylidene-1-tetralone;
In
water; dimethyl sulfoxide;
for 4.5h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/chem.201300557
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / ethanol / 24 h / Inert atmosphere; Schlenk technique
2.1: tetra-(n-butyl)ammonium iodide; potassium hydroxide / water; dimethyl sulfoxide / 0.75 h / Inert atmosphere; Schlenk technique
2.2: 4.5 h / Inert atmosphere; Schlenk technique
With
tetra-(n-butyl)ammonium iodide; potassium hydroxide;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1002/chem.201300557
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: chromium(VI) oxide; sulfuric acid / water; acetone / 1.5 h / Inert atmosphere; Schlenk technique; Cooling with ice
2.1: tetra-(n-butyl)ammonium iodide; potassium hydroxide / water; dimethyl sulfoxide / 0.75 h / Inert atmosphere; Schlenk technique
2.2: 4.5 h / Inert atmosphere; Schlenk technique
With
chromium(VI) oxide; sulfuric acid; tetra-(n-butyl)ammonium iodide; potassium hydroxide;
In
water; dimethyl sulfoxide; acetone;
DOI:10.1002/chem.201300557
