2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

Base Information

Chemical Name:2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene
CAS No.:172843-13-9
Molecular Formula:C₃₆H₅₆O₄Si
Molecular Weight:580.924
Hs Code.:

Synonyms:2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

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Technology Process of 2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

There total 3 articles about 2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 172843-11-7
3-O-tetradecanoyl-1-O-(tert-butyldiphenylsilyl)-1,3-dihydroxy-2-propanone

: 762-72-1
allyl-trimethyl-silane

: 172843-13-9
2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

Guidance literature:: With titanium tetrachloride; In dichloromethane; for 0.666667h; Ambient temperature;
DOI:10.1021/jm950276v

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 172843-13-9
2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / (dimethylamino)pyridine / pyridine / 16 h / Ambient temperature

2: 77 percent / DMAP, pyridine / CH₂Cl₂ / 24 h

3: 77 percent / TiCl₄ / CH₂Cl₂ / 0.67 h / Ambient temperature

With pyridine; dmap; titanium tetrachloride; In pyridine; dichloromethane;
DOI:10.1021/jm950276v

Reference yield:

: 172843-09-3
1-O-(tert-butyldiphenylsilyl)-1,3-dihydroxy-2-propanone

: 172843-13-9
2-hydroxy-2-<<(tert-butyldiphenylsilyl)oxy>methyl>-1-(tetradecanoyloxy)-4-pentene

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / DMAP, pyridine / CH₂Cl₂ / 24 h

2: 77 percent / TiCl₄ / CH₂Cl₂ / 0.67 h / Ambient temperature

With pyridine; dmap; titanium tetrachloride; In dichloromethane;
DOI:10.1021/jm950276v