C₂₇H₅₀O₄Si

Base Information

Chemical Name:C₂₇H₅₀O₄Si
CAS No.:1380510-97-3
Molecular Formula:C₂₇H₅₀O₄Si
Molecular Weight:466.777
Hs Code.:

C<sub>27</sub>H<sub>50</sub>O<sub>4</sub>Si

Synonyms:C₂₇H₅₀O₄Si

Suppliers and Price of C₂₇H₅₀O₄Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₇H₅₀O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₇H₅₀O₄Si

There total 12 articles about C₂₇H₅₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1380510-96-2
C₂₁H₃₆O₄

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1380510-97-3
C₂₇H₅₀O₄Si

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2012.04.030

Reference yield:

: Ender's imine

: 1380510-97-3
C₂₇H₅₀O₄Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: ozone / dichloromethane / -78 °C

2.1: dichloromethane / 2 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane / 3 h / 20 °C

4.1: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 24 h / 0 °C

5.1: dichloromethane / 1 h / 0 °C

6.1: diisobutylaluminium hydride / dichloromethane / 2 h / 20 °C

7.1: triethylamine / dichloromethane / 20 °C

8.1: potassium carbonate / methanol / 1 h / 20 °C

9.1: magnesium / tetrahydrofuran

9.2: 3 h / -35 °C

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 24 h / 110 °C

12.1: palladium 10% on activated carbon; hydrogen; sodium carbonate / ethyl acetate

13.1: lithium borohydride / tetrahydrofuran / 2 h / 0 - 20 °C

14.1: 1H-imidazole / dichloromethane / 0.5 h / 0 - 20 °C

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; potassium osmate(VI) dihydrate; lithium borohydride; methanesulfonamide; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; ozone; magnesium; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol; 4.1: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tetlet.2012.04.030

Reference yield:

: 1380510-76-8
C₉H₂₀O₃

: 1380510-97-3
C₂₇H₅₀O₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: dichloromethane / 1 h / 0 °C

2.1: diisobutylaluminium hydride / dichloromethane / 2 h / 20 °C

3.1: triethylamine / dichloromethane / 20 °C

4.1: potassium carbonate / methanol / 1 h / 20 °C

5.1: magnesium / tetrahydrofuran

5.2: 3 h / -35 °C

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 24 h / 110 °C

8.1: palladium 10% on activated carbon; hydrogen; sodium carbonate / ethyl acetate

9.1: lithium borohydride / tetrahydrofuran / 2 h / 0 - 20 °C

10.1: 1H-imidazole / dichloromethane / 0.5 h / 0 - 20 °C

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium borohydride; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene;
DOI:10.1016/j.tetlet.2012.04.030