(+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

Base Information

Chemical Name:(+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane
CAS No.:1092556-62-1
Molecular Formula:C₂₇H₄₆O₂SSi
Molecular Weight:462.813
Hs Code.:

Synonyms:(+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

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Technology Process of (+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

There total 1 articles about (+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 995-45-9
tributylchlorosilane

: 1092556-56-3
(-)-(6S,S(S))-(2E,4E)-5-(p-tolylsulfinyl)octa-2,4-dien-6-ol

: 1092556-62-1
(+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

Guidance literature:: With dmap; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jo801803m

Reference yield: 92.0%

: 1092556-62-1
(+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

: 1092556-65-4
(+)-(6S)-(2E,4E)-[5-(p-tolylsulfonyl)octa-2,4-dien-6-yloxy]tributylsilane

Guidance literature:: With magnesium bis(monoperoxyphthalate) hexahydrate; In methanol; at 0 - 20 ℃; for 7h; Inert atmosphere;
DOI:10.1021/jo801803m

Reference yield: 78.0%

: 1092556-62-1
(+)-(6S,S(S))-(2E,4E)-[5-(p-tolylsulfinyl)octa-2,4-dien-6-yloxy]tributylsilane

: 1092556-16-5
C₂₇H₄₆O₄SSi

Guidance literature:: With (-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III); ammonium acetate; dihydrogen peroxide; In methanol; dichloromethane; at 0 - 4 ℃; for 96h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo801803m