2-chlorothiobenzoic acid S-benzyl ester

Base Information

Chemical Name:2-chlorothiobenzoic acid S-benzyl ester
CAS No.:1333435-22-5
Molecular Formula:C₁₄H₁₁ClOS
Molecular Weight:262.76
Hs Code.:

Synonyms:2-chlorothiobenzoic acid S-benzyl ester

Suppliers and Price of 2-chlorothiobenzoic acid S-benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-chlorothiobenzoic acid S-benzyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-chlorothiobenzoic acid S-benzyl ester

There total 6 articles about 2-chlorothiobenzoic acid S-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2-chloro-benzoic acid-(4-chloro-benzyl ester)

: 100-53-8
phenylmethanethiol

: 1333435-22-5
2-chlorothiobenzoic acid S-benzyl ester

Guidance literature:: With [Bu₄N][Fe(CO)₃(NO)]; In 1,4-dioxane; at 20 - 80 ℃; for 12h; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201101073

Reference yield: 92.0%

: 89-98-5
2-chloro-benzaldehyde

: 100-53-8
phenylmethanethiol

: 1333435-22-5
2-chlorothiobenzoic acid S-benzyl ester

Guidance literature:: With 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; Phenazin; triethylamine; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c2cc17183j

Reference yield: 70.0%

: 49619-43-4
2-chlorobenzoic anhydride

: 100-39-0
benzyl bromide

: 1333435-22-5
2-chlorothiobenzoic acid S-benzyl ester

Guidance literature:: 2-chlorobenzoic anhydride; With Sodium thiosulfate pentahydrate; In N,N-dimethyl-formamide; at 70 ℃; for 1h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 70 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c8ob00178b