C₃₀H₃₄O₄Si

Base Information

Chemical Name:C₃₀H₃₄O₄Si
CAS No.:1360932-63-3
Molecular Formula:C₃₀H₃₄O₄Si
Molecular Weight:486.683
Hs Code.:

C<sub>30</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:C₃₀H₃₄O₄Si

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Chemical Property of C₃₀H₃₄O₄Si

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Technology Process of C₃₀H₃₄O₄Si

There total 6 articles about C₃₀H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1360932-61-1
C₃₀H₃₆O₅Si

: 124-63-0
methanesulfonyl chloride

: 1360932-63-3
C₃₀H₃₄O₄Si

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/chem.201102192

Reference yield:

: 1360932-59-7
C₂₅H₂₈O₄Si

: 1360932-63-3
C₃₀H₃₄O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid / toluene / 88 h / 20 °C

2: triethylamine / tetrahydrofuran / 0 - 20 °C

With (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; triethylamine; benzoic acid; In tetrahydrofuran; toluene;
DOI:10.1002/chem.201102192

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 1360932-63-3
C₃₀H₃₄O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 1 h / 0 °C

2.2: 3 h / 20 °C

3.1: aluminum (III) chloride; sodium iodide / dichloromethane; acetonitrile / 1 h / 0 °C

4.1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid / toluene / 88 h / 20 °C

5.1: triethylamine / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; aluminum (III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; triethylamine; benzoic acid; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201102192