3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

Base Information

Chemical Name:3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester
CAS No.:1026001-57-9
Molecular Formula:C₁₈H₂₈O₃S
Molecular Weight:324.485
Hs Code.:

Synonyms:3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

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Chemical Property of 3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

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Technology Process of 3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

There total 8 articles about 3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161392-19-4
3-Phenyl-thiopropionic acid S-{(R)-1-hexyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

: 1026001-57-9
3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 25 ℃; for 1h;
DOI:10.1021/jm00050a009

Reference yield:

: 111-25-1
1-bromo-hexane

: 1026001-57-9
3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) NaH / 1.) DMF, 45 min, 2.) DMF, 25 deg C, 14 h

2: 100 percent / 1 N HCl / methanol / 24 h / 25 °C

3: 92 percent / pyridine / tetrahydrofuran / 14 h / 25 °C

4: 71 percent / pyridine / CH₂Cl₂ / 14 h / 25 °C

5: 70 percent / dimethylformamide / 16 h / 80 °C

6: 100 percent / NaBH₄ / ethanol / 1 h / 55 °C

7: pyridine / 14 h / 25 °C

8: p-toluenesulfonic acid / CH₂Cl₂; methanol / 1 h / 25 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009

Reference yield:

: 86158-13-6
(2S)-3-(hexyloxy)-1,2-propanediol

: 1026001-57-9
3-Phenyl-thiopropionic acid S-((S)-2-hexyloxy-1-hydroxymethyl-ethyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / pyridine / tetrahydrofuran / 14 h / 25 °C

2: 71 percent / pyridine / CH₂Cl₂ / 14 h / 25 °C

3: 70 percent / dimethylformamide / 16 h / 80 °C

4: 100 percent / NaBH₄ / ethanol / 1 h / 55 °C

5: pyridine / 14 h / 25 °C

6: p-toluenesulfonic acid / CH₂Cl₂; methanol / 1 h / 25 °C

With pyridine; sodium tetrahydroborate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009