2-iodo-4-phenethylbenzoic acid

Base Information

Chemical Name:2-iodo-4-phenethylbenzoic acid
CAS No.:910240-74-3
Molecular Formula:C₁₅H₁₃IO₂
Molecular Weight:352.172
Hs Code.:

Synonyms:2-iodo-4-phenethylbenzoic acid

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Chemical Property of 2-iodo-4-phenethylbenzoic acid

Chemical Property:

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Technology Process of 2-iodo-4-phenethylbenzoic acid

There total 6 articles about 2-iodo-4-phenethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910240-72-1
2-amino-4-phenethylbenzoic acid

: 910240-74-3
2-iodo-4-phenethylbenzoic acid

Guidance literature:: 2-amino-4-phenethylbenzoic acid; With hydrogenchloride; acetic acid; sodium nitrite; In water; at 4 ℃; for 0.25h;

With potassium iodide; In water; at 4 - 20 ℃; for 0.5h;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 910240-74-3
2-iodo-4-phenethylbenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate / palladium diacetate; tetrabutylammomium bromide / ISOPROPYLAMIDE / 6 h / 20 - 110 °C

2.1: hydrogen / 5%-palladium/activated carbon / methanol; ethyl acetate / 2 h / 20 °C

3.1: trifluoroacetic acid / 16 h / 20 °C

3.2: pH 6.4

4.1: hydrogenchloride; acetic acid; sodium nitrite / water / 0.25 h / 4 °C

4.2: 0.5 h / 4 - 20 °C

With hydrogenchloride; hydrogen; sodium acetate; acetic acid; trifluoroacetic acid; sodium nitrite; palladium diacetate; 5%-palladium/activated carbon; tetrabutylammomium bromide; In methanol; ISOPROPYLAMIDE; water; ethyl acetate;

Reference yield:

: 890315-79-4
tert-butyl 2-nitro-4-((E)-2-phenylvinyl)benzoate

: 910240-74-3
2-iodo-4-phenethylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / 5%-palladium/activated carbon / methanol; ethyl acetate / 2 h / 20 °C

2.1: trifluoroacetic acid / 16 h / 20 °C

2.2: pH 6.4

3.1: hydrogenchloride; acetic acid; sodium nitrite / water / 0.25 h / 4 °C

3.2: 0.5 h / 4 - 20 °C

With hydrogenchloride; hydrogen; acetic acid; trifluoroacetic acid; sodium nitrite; 5%-palladium/activated carbon; In methanol; water; ethyl acetate;