2-acetamido-9,9-dimethylfluorene

Base Information

Chemical Name:2-acetamido-9,9-dimethylfluorene
CAS No.:63021-04-5
Molecular Formula:C₁₇H₁₇NO
Molecular Weight:251.328
Hs Code.:

Synonyms:2-acetamido-9,9-dimethylfluorene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-acetamido-9,9-dimethylfluorene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-acetamido-9,9-dimethylfluorene

There total 1 articles about 2-acetamido-9,9-dimethylfluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4569-45-3
9,9-dimethyl-9H-fluorene

: 63021-04-5
2-acetamido-9,9-dimethylfluorene

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; HNO₃

2: zinc; acetic acid; CaCl₂ / in wss.Aethanol, und Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin

With nitric acid; acetic acid; calcium chloride; zinc;
DOI:10.1002/hlca.19530360635

Reference yield:

: 63021-04-5
2-acetamido-9,9-dimethylfluorene

: 108714-73-4
9,9-dimethyl-9H-fluoren-2-ylamine

Guidance literature:: With water; potassium hydroxide; In ethanol; xylene; for 36h; Product distribution / selectivity; Reflux;

Reference yield:

: 63021-04-5
2-acetamido-9,9-dimethylfluorene

: 1260228-95-2
12,12-dimethyl-11,12-dihydroindeno[2,1-a]carbazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid / propionic acid / 1 h / -15 °C

2.1: hydrogenchloride / ethanol / 3 h / 115 °C

3.1: hydrogenchloride; sodium nitrite / dimethyl sulfoxide; water / 2.5 h / -5 - 25 °C

3.2: 20 h / -5 - 28 °C

4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene / 24 h / Inert atmosphere; Reflux

5.1: triphenylphosphine / 1,2-dichloro-benzene / 16 h / 195 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; nitric acid; potassium carbonate; triphenylphosphine; sodium nitrite; In ethanol; water; dimethyl sulfoxide; propionic acid; 1,2-dichloro-benzene; toluene; 4.1: |Suzuki Coupling;