3-amino-9,9’-dimethylfluorene

Base Information

Chemical Name:3-amino-9,9’-dimethylfluorene
CAS No.:1421789-14-1
Molecular Formula:C₁₅H₁₅N
Molecular Weight:209.291
Hs Code.:

Synonyms:

Suppliers and Price of 3-amino-9,9’-dimethylfluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 10 raw suppliers

Chemical Property of 3-amino-9,9’-dimethylfluorene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-amino-9,9’-dimethylfluorene

There total 4 articles about 3-amino-9,9’-dimethylfluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9,9-dimethyl-3-nitro-9H-fluorene

: 1421789-14-1
3-amino-9,9’-dimethylfluorene

Guidance literature:: With aluminum (III) chloride; iron; In 1,4-dioxane; for 8h; Reflux;

Reference yield:

: 63021-04-5
2-acetamido-9,9-dimethylfluorene

: 1421789-14-1
3-amino-9,9’-dimethylfluorene

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; sulfuric acid / 2 h / 5 - 10 °C

2: potassium hydroxide / ethanol / 4 h / Reflux

3: hypophosphoric acid; sodium nitrite; sulfuric acid / water; tetrahydrofuran / 0 - 10 °C

4: iron; aluminum (III) chloride / 1,4-dioxane / 8 h / Reflux

With aluminum (III) chloride; sulfuric acid; nitric acid; iron; hypophosphoric acid; potassium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; ethanol; water;

Reference yield:

: 108714-73-4
9,9-dimethyl-9H-fluoren-2-ylamine

: 1421789-14-1
3-amino-9,9’-dimethylfluorene

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 3 h

2: nitric acid; sulfuric acid / 2 h / 5 - 10 °C

3: potassium hydroxide / ethanol / 4 h / Reflux

4: hypophosphoric acid; sodium nitrite; sulfuric acid / water; tetrahydrofuran / 0 - 10 °C

5: iron; aluminum (III) chloride / 1,4-dioxane / 8 h / Reflux

With aluminum (III) chloride; sulfuric acid; nitric acid; iron; hypophosphoric acid; potassium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;