2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

Base Information

Chemical Name:2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide
CAS No.:1454928-17-6
Molecular Formula:C₂₂H₂₈BrN₃O₂
Molecular Weight:446.387
Hs Code.:

Synonyms:2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

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Chemical Property of 2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

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Technology Process of 2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

There total 1 articles about 2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 35656-89-4
4-(4-bromophenyl)butanoic acid

: 1-(4-(tert-butyl)benzyl)hydrazinecarboxamide monomethanesulfonate

: 1454928-17-6
2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield: 57.0%

: 1454928-17-6
2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

: 1454928-18-7
3-(3-(4-bromophenyl)propyl)-1-(4-(tert-butyl)benzyl)-1H-1,2,4-triazol-5(4H)-one

Guidance literature:: With camphor-10-sulfonic acid; In ethyl acetate; at 80 ℃; for 16h;

Reference yield:

: 1454928-17-6
2-(4-(4-bromophenyl)butanoyl)-1-(4-(tert-butyl)benzyl)hydrazinecarboxamide

: 1454927-31-1
1-(4-(tert-butyl)benzyl)-3-(3-(4'-(3-hydroxyoxetan-3-yl)-[1,1'-biphenyl]-4-yl)propyl)-1H-1,2,4-triazol-5(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / ethyl acetate / 16 h / 80 °C

2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; water / 1,2-dimethoxyethane / 18 h / 110 °C / Inert atmosphere; Sealed tube

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; camphor-10-sulfonic acid; water; In 1,2-dimethoxyethane; ethyl acetate;