bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine

Base Information

Chemical Name:bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine
CAS No.:90215-35-3
Molecular Formula:C₃₀H₂₆FeN₈O₄
Molecular Weight:618.435
Hs Code.:

Synonyms:bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine

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Technology Process of bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine

There total 3 articles about bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-monohydrate

: 90215-35-3
bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine

Guidance literature:: With pyridine; In pyridine; educt and pyridine stirred for 24 h; product filtered off, washed with Et2O, dried at 30°C/0.1 mm; elem. anal.;
DOI:10.1016/S0277-5387(00)81515-6

Reference yield:

: 1080-89-3
4-hydroxyimino-3-methyl-1-phenyl-2-pyrazolin-5-one

: 90215-35-3
bis(3-methyl-1-phenyl-4-oximato-1H-pyrazole-4,5-dione)iron(II)-dipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: water / water; ethanol

2: pyridine / pyridine

With water; pyridine; In pyridine; ethanol; water;
DOI:10.1016/S0277-5387(00)81515-6

Reference yield:

: Ammonium iron sulfate

: 440362-10-7
4-oximino-1-phenyl-3-methyl-2-pyrazolin-5-one

: 90215-35-3
Fe(C₆H₅C₃N₂(CH₃)NOO)2(C₅H₅N)2

Guidance literature:: With pyridine; In ethanol; water; org. compound in hot ethanol containing pyridine was added dropwise to a soln. of Co-salt in water under stirring; filtered, washed (cold water, ethanol), dried in air; elem. anal.;