(2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

Base Information

Chemical Name:(2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine
CAS No.:1172121-98-0
Molecular Formula:C₁₉H₂₈O₄
Molecular Weight:320.429
Hs Code.:

Synonyms:(2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

Suppliers and Price of (2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

There total 1 articles about (2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1172121-96-8
(2R,8S,9R)-8-benzyloxy-9-(tert-butyldiphenylsilanyloxymethyl)-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

: 1172121-98-0
(2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

Guidance literature:: (2R,8S,9R)-8-benzyloxy-9-(tert-butyldiphenylsilanyloxymethyl)-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 18.5h; Inert atmosphere;

With water; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.tetasy.2009.03.010

Reference yield: 86.0%

: 1172121-98-0
(2R,8S,9R)-8-benzyloxy-9-hydroxymethyl-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine

: 1172121-99-1
(2R,8S,9S)-8-benzyloxy-2-methoxy-2-vinyl-2,3,4,5,6,7,8,9-octahydrooxonine-2-carbaldehyde

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 1.33333h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.03.010