6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

Base Information

Chemical Name:6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline
CAS No.:1401971-47-8
Molecular Formula:C₂₄H₂₂N₄O₃
Molecular Weight:414.464
Hs Code.:

Synonyms:6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

Suppliers and Price of 6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

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Technology Process of 6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

There total 1 articles about 6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 5444-01-9
3-cyano-4-methylpyridine

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1401971-47-8
6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

Guidance literature:: With potassium tert-butylate; at 35 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2012.08.047

Reference yield: 75.0%

: 1401971-47-8
6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

: 1401971-80-9
6-amino-11-(3,4,5-trimethoxyphenyl)pyrido[3,4-c][1,9]phenanthroline

Guidance literature:: With palladium 10% on activated carbon; for 0.166667h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.08.047

Reference yield:

: 1401971-47-8
6-amino-11-(3,4,5-trimethoxyphenyl)-11,12-dihydropyrido[3,4-c][1,9]phenanthroline

: 11-(3,4,5-trimethoxyphenyl)-5,6-dihydropyrido[3,4-c][1,9]phenanthrolin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon / 0.17 h / Inert atmosphere; Reflux

2: sulfuric acid; sodium nitrite; hypophosphorous acid; acetic acid; copper(II) sulfate / water / 1 h / 0 °C

With sulfuric acid; palladium 10% on activated carbon; hypophosphorous acid; copper(II) sulfate; acetic acid; sodium nitrite; In water;
DOI:10.1002/cmdc.201700026