Technology Process of C14H9F3N2S
There total 5 articles about C14H9F3N2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; iron / ethanol; water / 1.75 h / 150 °C / Microwave irradiation
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 20 °C / Inert atmosphere
3.1: N-chloro-succinimide / dichloromethane / 18 h / -78 - 20 °C
4.1: toluene / 12 h / Reflux
With
N-chloro-succinimide; iron; acetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1039/c3ce42205d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere
1.2: 18 h / 20 °C / Inert atmosphere
2.1: N-chloro-succinimide / dichloromethane / 18 h / -78 - 20 °C
3.1: toluene / 12 h / Reflux
With
N-chloro-succinimide; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c3ce42205d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-chloro-succinimide / dichloromethane / 18 h / -78 - 20 °C
2: toluene / 12 h / Reflux
With
N-chloro-succinimide;
In
dichloromethane; toluene;
DOI:10.1039/c3ce42205d
