trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

Base Information

• Chemical Name: trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid
• CAS No.: 121618-26-6
• Molecular Formula: C₈H₃Cl₃F₆O
• Molecular Weight: 335.461

Synonyms:trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

Chemical Property of trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

Chemical Property:

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Technology Process of trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

There total 2 articles about trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl (dimethylsulfuranylidene)acetate (7380-81-6) + 1,1-Dichlor-5,5,5-trifluor-4-(trifluormethyl)-1,3-pentadien (99903-40-9) → dimethylsulfide (75-18-3) + trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (121618-26-6) + (1S,3S)-3-(2,2-Dichloro-vinyl)-2,2-bis-trifluoromethyl-cyclopropanecarbonyl chloride (121618-26-6)

Guidance literature:

Multistep reaction. Title compound not separated from byproducts;

Reference yield:

ethyl (dimethylsulfuranylidene)acetate (7380-81-6) + 1,1-Dichlor-5,5,5-trifluor-4-(trifluormethyl)-1,3-pentadien (99903-40-9) → dimethylsulfide (75-18-3) + trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (121618-26-6) + (1S,3S)-3-(2,2-Dichloro-vinyl)-2,2-bis-trifluoromethyl-cyclopropanecarbonyl chloride (121618-26-6)

Guidance literature:

Multistep reaction. Title compound not separated from byproducts;

Reference yield: 85.0%

2-hydroxy-2-(3-phenoxyphenyl)acetonitrile (39515-47-4) + trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (121618-26-6) → trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeure-(α-cyan-3-phenoxybenzyl)ester (82224-37-1,102778-61-0,102779-31-7,121701-43-7,121701-46-0)

Guidance literature:

With pyridine; In toluene; for 72h; Ambient temperature;

upstream raw materials:

ethyl (dimethylsulfuranylidene)acetate

1,1-Dichlor-5,5,5-trifluor-4-(trifluormethyl)-1,3-pentadien

Downstream raw materials:

trans-3-(2,2-Dichlorvinyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeure-(α-cyan-3-phenoxybenzyl)ester

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