Technology Process of C20H23FN4O4S
There total 6 articles about C20H23FN4O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
morpholine; sulfur;
In
ethanol;
at 100 ℃;
for 0.583333h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; sodium nitrite / ethanol; water / 0.33 h / 0 °C
1.2: 2 h / 0 °C
2.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation
3.1: sodium hydroxide; water / ethanol / 16 h / 20 °C
3.2: pH 2
4.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 5 h / 0 - 100 °C
5.1: sodium hydride / N,N-dimethyl-formamide / 12 h / 95 °C
6.1: sulfur; morpholine / ethanol / 0.58 h / 100 °C / Microwave irradiation
With
morpholine; hydrogenchloride; diphenyl phosphoryl azide; ammonium acetate; water; sodium hydride; sulfur; acetic acid; triethylamine; sodium hydroxide; sodium nitrite;
In
ethanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation
2.1: sodium hydroxide; water / ethanol / 16 h / 20 °C
2.2: pH 2
3.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 5 h / 0 - 100 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 12 h / 95 °C
5.1: sulfur; morpholine / ethanol / 0.58 h / 100 °C / Microwave irradiation
With
morpholine; diphenyl phosphoryl azide; ammonium acetate; water; sodium hydride; sulfur; acetic acid; triethylamine; sodium hydroxide;
In
ethanol; N,N-dimethyl-formamide;