(S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

Base Information

Chemical Name:(S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide
CAS No.:449728-89-6
Molecular Formula:C₃₃H₄₁N₃O₄
Molecular Weight:543.706
Hs Code.:

Synonyms:(S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

Chemical Property:

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Technology Process of (S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

There total 4 articles about (S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 251304-81-1
8-((benzyloxy)amino)-8-oxooctanoic acid

: (S)-2-amino-3-phenyl-N-(3-phenyl-propyl)propionamide tosylate

: 449728-89-6
(S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm0208119

Reference yield:

: 3946-32-5
suberic acid monomethyl ester

: 449728-89-6
(S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

2: 68 percent / aq. LiOH / tetrahydrofuran / 20 °C

3: 52 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

With lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0208119

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 449728-89-6
(S)-octanedioic acid benzyloxy-amide [2-phenyl-1-(3-phenyl-propylcarbamoyl)ethyl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

2: 68 percent / aq. LiOH / tetrahydrofuran / 20 °C

3: 52 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

With lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0208119