(Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

Base Information

Chemical Name:(Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid
CAS No.:91632-55-2
Molecular Formula:C₁₉H₁₆N₂O₂
Molecular Weight:304.348
Hs Code.:

Synonyms:(Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

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Chemical Property of (Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

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Technology Process of (Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

There total 4 articles about (Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 91632-37-0
4,4'-Di-p-tolyl-4'H-[2,4']biisoxazolyl-5,5'-dione

: 91632-55-2
(Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

Guidance literature:: In tetrahydrofuran; for 0.5h; Heating;
DOI:10.1021/jo00196a034

Reference yield:

: 14062-19-2
p-tolylacetic acid ethyl ester

: 91632-55-2
(Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / NaH (80percent suspension) / 2.5 h / Ambient temperature

2: 70 percent / NH₂OH*HCl / H₂O; methanol / 1 h / Heating

3: 90 percent / 30percent H₂O₂/HCOOH

4: 89 percent / tetrahydrofuran / 0.5 h / Heating

With formic acid; hydroxylamine hydrochloride; dihydrogen peroxide; sodium hydride; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo00196a034

Reference yield:

: 91632-29-0
4-p-Tolyl-2H-isoxazol-5-one

: 91632-55-2
(Z)-3-{[1-Cyano-1-p-tolyl-meth-(Z)-ylidene]-amino}-2-p-tolyl-acrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 30percent H₂O₂/HCOOH

2: 89 percent / tetrahydrofuran / 0.5 h / Heating

With formic acid; dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1021/jo00196a034