N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

Base Information

Chemical Name:N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione
CAS No.:1078120-40-7
Molecular Formula:C₂₃H₁₆N₂O₂S
Molecular Weight:384.458
Hs Code.:

Synonyms:N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

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Chemical Property of N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

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Technology Process of N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

There total 6 articles about N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1078120-16-7
N-benzyl-N-(4-methoxyphenyl)-3-phenylpropiolamide

: 1701-93-5
silver thiocyanate

: 1078120-40-7
N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

Guidance literature:: With ammonium cerium (IV) nitrate; In dimethyl sulfoxide; at 60 ℃; for 0.5h;
DOI:10.1021/acs.joc.0c02270

Reference yield: 75.0%

: 1078120-16-7
N-benzyl-N-(4-methoxyphenyl)-3-phenylpropiolamide

: 1147550-11-5
ammonium thiocyanate

: 1078120-40-7
N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

Guidance literature:: With carbon nitride g-C₃N₄; air; at 20 ℃; for 12h; Irradiation; Green chemistry;
DOI:10.1039/d1gc00938a

Reference yield: 57.0%

: 1078120-16-7
N-benzyl-N-(4-methoxyphenyl)-3-phenylpropiolamide

: 1111-67-7,15192-76-4,26656-82-6
copper(I) thiocyanate

: 1078120-40-7
N-benzyl-3-thiocyanato-4-phenyl-1-azaspiro[4,5]deca-3,6,9-triene-2,8-dione

Guidance literature:: With 1-Chloromethyl-4-methyl-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate); In acetonitrile; at 90 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jo8018297