Technology Process of C26H36O2
There total 10 articles about C26H36O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: camphor-10-sulfonic acid / dichloromethane; methanol / 1.5 h / 20 °C / Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C / Inert atmosphere
3.2: 3 h / 0 - 20 °C / Inert atmosphere
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
5.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
6.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C / Inert atmosphere
6.2: 0 - 20 °C / Inert atmosphere
7.1: toluene / 20 h / 110 °C / Inert atmosphere
With
lithium aluminium tetrahydride; camphor-10-sulfonic acid; sodium hydride; Dess-Martin periodane;
In
tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
3.2: |Horner-Wadsworth-Emmons Olefination / 6.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1002/chem.201201585
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C / Inert atmosphere
1.2: 3 h / 0 - 20 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
3.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C / Inert atmosphere
4.2: 0 - 20 °C / Inert atmosphere
5.1: toluene / 20 h / 110 °C / Inert atmosphere
With
lithium aluminium tetrahydride; sodium hydride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
1.2: |Horner-Wadsworth-Emmons Olefination / 4.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1002/chem.201201585