2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate

Base Information

• Chemical Name: 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate
• CAS No.: 497949-72-1
• Molecular Formula: C₁₇H₁₇ClN₂O₇S
• Molecular Weight: 428.85
• Mol file: 497949-72-1.mol

Synonyms:2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate

Chemical Property of 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate

Chemical Property:

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Technology Process of 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate

There total 1 articles about 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

isocyanate de chlorosulfonyle (1189-71-5) + 4-chloro-aniline (106-47-8) + 2-methoxycarbonylmethoxybenzyl alcohol (128001-41-2) → 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate (497949-72-1)

Guidance literature:

isocyanate de chlorosulfonyle; 2-methoxycarbonylmethoxybenzyl alcohol; In tetrahydrofuran; at -5 ℃; for 0.5h;

4-chloro-aniline; In tetrahydrofuran; for 2h; Further stages.;

DOI:10.1021/ol0272489

Reference yield: 51.0%

1,3,5-trimethyl-benzene (108-67-8) + 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate (497949-72-1) → methyl 2-[2-(2,4,6-trimethylbenzyl)-phenoxy]-acetate

Guidance literature:

at 130 ℃; for 5h;

DOI:10.1021/ol0272489

Reference yield:

m-xylene (108-38-3,104809-90-7) + 2-methoxycarbonylmethoxybenzyl N-(4-chlorophenyl)-sulfamoylcarbamate (497949-72-1) → methyl 2-(2,6-dimethylbenzyl)phenoxy-acetate + methyl 2-(2,4-dimethylbenzyl)phenoxy-acetate

Guidance literature:

at 138 ℃; Title compound not separated from byproducts.;

DOI:10.1021/ol0272489

upstream raw materials:

isocyanate de chlorosulfonyle

4-chloro-aniline

2-methoxycarbonylmethoxybenzyl alcohol