3-hydroxy-5-chlorophenyl acetic acid

Base Information

• Chemical Name: 3-hydroxy-5-chlorophenyl acetic acid
• CAS No.: 149029-88-9
• Molecular Formula: C₈H₇ClO₃
• Molecular Weight: 186.595

Synonyms:3-hydroxy-5-chlorophenyl acetic acid

Chemical Property of 3-hydroxy-5-chlorophenyl acetic acid

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-hydroxy-5-chlorophenyl acetic acid

There total 2 articles about 3-hydroxy-5-chlorophenyl acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C10H11ClO3 (825645-06-5) → 3-hydroxy-5-chlorophenyl acetic acid (149029-88-9)

Guidance literature:

With water; hydrogen bromide; acetic acid; for 22h; Reflux;

DOI:10.1016/j.bmcl.2009.09.052

Reference yield:

(3-chloro-5-methoxyphenyl)acetonitrile (178486-31-2) → 3-hydroxy-5-chlorophenyl acetic acid (149029-88-9)

Guidance literature:

With tetrabutyl-ammonium chloride; water; hydrogen bromide; at 125 ℃; for 36h;

Reference yield:

2-chloro-1-fluoro-4-(methylsulfonyl)benzene (847148-17-8) + 3-hydroxy-5-chlorophenyl acetic acid (149029-88-9) → {3-chloro-5-[2-chloro-4-(methylsulfonyl)phenoxy]phenyl}acetic acid (934241-05-1)

Guidance literature:

With caesium carbonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 5h;

upstream raw materials:

(3-chloro-5-methoxyphenyl)acetonitrile

C₁₀H₁₁ClO₃

Downstream raw materials:

{3-chloro-5-[2-chloro-4-(methylsulfonyl)phenoxy]phenyl}acetic acid

C₁₇H₁₅ClN₂O₆

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