tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate

Base Information

• Chemical Name: tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate
• CAS No.: 1605320-74-8
• Molecular Formula: C₁₄H₄₁NO₆P₂Si₄
• Molecular Weight: 493.772
• Mol file: 1605320-74-8.mol

Synonyms:tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate

Chemical Property of tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate

There total 1 articles about tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

tris(trimethylsilyl) phosphite (1795-31-9) + ethyl acetimidate hydrochloride (2208-07-3) → tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate (1605320-74-8)

Guidance literature:

tris(trimethylsilyl) phosphite; ethyl acetimidate hydrochloride; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 1h; Reflux;

With 1,1,1,3,3,3-hexamethyl-disilazane; for 1h; Reflux;

DOI:10.1134/S1070363214030347

Reference yield: 98.0%

tetrakis(trimethylsilyl) (1-aminoethane-1,1-diyl) bisphosphonate (1605320-74-8) → 1-amino-ethane-1,1-diphosphonic acid (15049-85-1)

Guidance literature:

With methanol; In diethyl ether; Reflux;

DOI:10.1007/s11172-016-1289-z

upstream raw materials:

tris(trimethylsilyl) phosphite

ethyl acetimidate hydrochloride

Downstream raw materials:

1-amino-ethane-1,1-diphosphonic acid