dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

Base Information

Chemical Name:dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron
CAS No.:121919-41-3
Molecular Formula:C₂₄H₂₀FeO₂Si
Molecular Weight:424.354
Hs Code.:

Synonyms:dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

Suppliers and Price of dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

There total 1 articles about dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 1-chloro-1-methyl-2,5-diphenylsilole

: 121919-41-3
dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

Guidance literature:: With sodium amalgam; In tetrahydrofuran; under N2, addn. of a soln. of Na(Fe(CO)2(C5H5)) (prpd. from (Fe(CO)2(C5H5))2 and Na#Hg in THF) to a stirred soln. of the silole at -78°C, warming to room temp., stirring 12 h; vac. evapn., dissoln. in a mininimum amt. of toluene, column chromy. on acidic alumina (toluene/hexane, 1/1), concn. to ca. 20 ml, cooling to -78 °C (pptn.), recrystn. from CH2Cl2/hexane at -20 °C, elem. anal.;

Reference yield: 48.0%

: 121919-41-3
dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

: 12129-70-3
carbonyhltungsten⁽⁰⁾(cycloocta-1,5-diene)

: 121962-47-8
cis-dicarbonylbis{η4-exo-1-(dicarbonyl(η5-cyclopentadienyl)ferrio)-endo-1-methyl-2.5-diphenylsilole}tungesten*2(toluene)

Guidance literature:: In octane; under N2, refluxing 8 h; vac. evapn., extn. with hexane (2x), vac. evapn., chromy on silica gel column (toluene/hexane, 9/1), the red soln. left at -20°C (pptn.), elem. anal.;

Reference yield: 39.0%

: 15321-51-4
diiron nonacarbonyl

: 121919-41-3
dicarbonyl(η5-cyclopentadienyl)(1-methyl-2,5-diphenylsilacyclopentadien-1-yl)iron

: 121919-45-7
tricarbonyl{η4-exo-1-(dicarbonyl(η5-cyclopentadienyl)ferrio)-endo-1-methyl-2,5-diphenylsilole}iron

Guidance literature:: In benzene; under N2, heating at 65 °C, 16 h; vac. evapn., extn. with hexane, filtration, the red soln. left at -78°C (pptn.), elem. anal.;