C₃₉H₅₇NO₁₂Si

Base Information

Chemical Name:C₃₉H₅₇NO₁₂Si
CAS No.:1007094-41-8
Molecular Formula:C₃₉H₅₇NO₁₂Si
Molecular Weight:759.967
Hs Code.:

C<sub>39</sub>H<sub>57</sub>NO<sub>12</sub>Si

Synonyms:C₃₉H₅₇NO₁₂Si

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Chemical Property of C₃₉H₅₇NO₁₂Si

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Technology Process of C₃₉H₅₇NO₁₂Si

There total 6 articles about C₃₉H₅₇NO₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848251-62-7
C₃₆H₅₂O₁₁Si

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1007094-41-8
C₃₉H₅₇NO₁₂Si

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -40 ℃;
DOI:10.1016/j.jfluchem.2008.05.013

Reference yield:

: 32981-86-5,172018-16-5
10-deacetylbaccatin III

: 1007094-41-8
C₃₉H₅₇NO₁₂Si

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / -10 °C

3: diisopropyl-carbodiimide; dmap / dichloromethane

4: pyridine; hydrogen fluoride / acetonitrile

5: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

6: lithium hexamethyldisilazane / tetrahydrofuran

With pyridine; 1H-imidazole; dmap; hydrogen fluoride; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium hexamethyldisilazane; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.jfluchem.2012.07.007

Reference yield:

: 194720-19-9
7,10,13-tris(triethylsilyl)-10-deacetylbaccatin III

: 1007094-41-8
C₃₉H₅₇NO₁₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / -10 °C

2: diisopropyl-carbodiimide; dmap / dichloromethane

3: pyridine; hydrogen fluoride / acetonitrile

4: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

5: lithium hexamethyldisilazane / tetrahydrofuran

With pyridine; 1H-imidazole; dmap; hydrogen fluoride; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium hexamethyldisilazane; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.jfluchem.2012.07.007