C₄₉H₆₉O₁₄P

Base Information

• Chemical Name: C₄₉H₆₉O₁₄P
• CAS No.: 170707-06-9
• Molecular Formula: C₄₉H₆₉O₁₄P
• Molecular Weight: 913.052
• Mol file: 170707-06-9.mol

Synonyms:C₄₉H₆₉O₁₄P

Chemical Property of C₄₉H₆₉O₁₄P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₉H₆₉O₁₄P

There total 21 articles about C₄₉H₆₉O₁₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C45H62O10 (161984-90-3) → C49H69O14P (170707-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / pyridine / CH₂Cl₂ / 0.25 h / 0 °C

2: 4 h / 90 °C

With pyridine; In dichloromethane;

DOI:10.1021/ja00146a010

Reference yield:

C45H62O9 (161984-86-7) → C49H69O14P (170707-06-9)

Guidance literature:

Multi-step reaction with 8 steps

1: 435 mg / pyridinium p-toluenesulfonate / CH₂Cl₂ / 14 h / 0 °C

2: 2,6-lutidine / CH₂Cl₂ / 0.25 h / 0 °C

3: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, 25 deg C, 1 h

4: tetrahydrofuran / 0.5 h / 0 °C

5: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 25 °C

6: 90 percent / TBAF / tetrahydrofuran / 2 h / 25 °C

7: 81 percent / pyridine / CH₂Cl₂ / 0.25 h / 0 °C

8: 4 h / 90 °C

With pyridine; 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; Dess-Martin periodane; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00146a010

Reference yield:

C45H62O9 (170707-12-7) → C49H69O14P (170707-06-9)

Guidance literature:

Multi-step reaction with 7 steps

1: 2,6-lutidine / CH₂Cl₂ / 0.25 h / 0 °C

2: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, 25 deg C, 1 h

3: tetrahydrofuran / 0.5 h / 0 °C

4: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 25 °C

5: 90 percent / TBAF / tetrahydrofuran / 2 h / 25 °C

6: 81 percent / pyridine / CH₂Cl₂ / 0.25 h / 0 °C

7: 4 h / 90 °C

With pyridine; 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; Dess-Martin periodane; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00146a010

upstream raw materials:

C₄₇H₆₃BrO₁₁

phosphorous acid trimethyl ester

C₄₅H₆₂O₉

C₄₅H₆₂O₉

Downstream raw materials:

C₄₇H₆₂O₁₀

C₄₀H₅₈O₁₁S

C₄₇H₆₄O₉