Technology Process of C49H69O14P
There total 21 articles about C49H69O14P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 81 percent / pyridine / CH2Cl2 / 0.25 h / 0 °C
2: 4 h / 90 °C
With
pyridine;
In
dichloromethane;
DOI:10.1021/ja00146a010
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 435 mg / pyridinium p-toluenesulfonate / CH2Cl2 / 14 h / 0 °C
2: 2,6-lutidine / CH2Cl2 / 0.25 h / 0 °C
3: 1.) O3, 2.) Ph3P / 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, 25 deg C, 1 h
4: tetrahydrofuran / 0.5 h / 0 °C
5: Dess-Martin periodinane / CH2Cl2 / 2 h / 25 °C
6: 90 percent / TBAF / tetrahydrofuran / 2 h / 25 °C
7: 81 percent / pyridine / CH2Cl2 / 0.25 h / 0 °C
8: 4 h / 90 °C
With
pyridine; 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; Dess-Martin periodane; ozone; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00146a010
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 2,6-lutidine / CH2Cl2 / 0.25 h / 0 °C
2: 1.) O3, 2.) Ph3P / 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, 25 deg C, 1 h
3: tetrahydrofuran / 0.5 h / 0 °C
4: Dess-Martin periodinane / CH2Cl2 / 2 h / 25 °C
5: 90 percent / TBAF / tetrahydrofuran / 2 h / 25 °C
6: 81 percent / pyridine / CH2Cl2 / 0.25 h / 0 °C
7: 4 h / 90 °C
With
pyridine; 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; Dess-Martin periodane; ozone; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00146a010
