2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

Base Information

Chemical Name:2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine
CAS No.:590418-90-9
Molecular Formula:C₃₂H₄₄NP
Molecular Weight:473.682
Hs Code.:

2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-<i>tert</i>-butyl-pyridine

Synonyms:2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

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Chemical Property of 2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

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Technology Process of 2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

There total 2 articles about 2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 67950-05-4
bis(2,4,6-trimethylphenyl)chlorophosphine

: 102348-41-4
2,4-di-tert-butyl-6-methylpyridine

: 590418-90-9
2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 3h;
DOI:10.1039/b212169g

Reference yield:

: 109-06-8
α-picoline

: 590418-90-9
2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / nBuLi / hexane; tetrahydrofuran / 3 h / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1039/b212169g

Reference yield: 92.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 590418-90-9
2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

: 590418-92-1
(PdClCH₃P(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)2)2

Guidance literature:: In dichloromethane; a mixt. in CH2cl2 was stirred at ambient temp. for 1 h (N2); concd., washed with hexane; elem. anal.;
DOI:10.1039/b212169g