2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Base Information

Chemical Name:2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide
CAS No.:59892-57-8
Molecular Formula:C₂₀H₂₀BrNO₆
Molecular Weight:450.286
Hs Code.:

Synonyms:2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Suppliers and Price of 2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

There total 6 articles about 2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 59892-56-7
methyl 2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-β-D-xylo-hexopyranoside

: 59892-57-8
2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Guidance literature:: With hydrogen bromide; In dichloromethane; at -20 ℃; for 1.75h;

Reference yield:

: 59892-66-9
3,6-dideoxy-2,4-di-O-(p-nitrobenzoyl)-α-D-xylo-hexopyranosyl bromide

: 59892-57-8
2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: silver carbonate / CH₂Cl₂ / 16 h

2: 47 percent / K₂CO₃ / methanol / 1.25 h / 0 °C

3: 88 percent / silver oxide / toluene / 48 h / 20 °C / in the dark

4: 100 percent / HBr / CH₂Cl₂ / 1.75 h / -20 °C

With hydrogen bromide; potassium carbonate; silver carbonate; silver(l) oxide; In methanol; dichloromethane; toluene;

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 59892-57-8
2-O-benzyl-3,6-dideoxy-4-O-p-nitrobenzoyl-α-D-xylo-hexopyranosyl bromide

Guidance literature:: Multi-step reaction with 5 steps

2: silver carbonate / CH₂Cl₂ / 16 h

3: 47 percent / K₂CO₃ / methanol / 1.25 h / 0 °C

4: 88 percent / silver oxide / toluene / 48 h / 20 °C / in the dark

5: 100 percent / HBr / CH₂Cl₂ / 1.75 h / -20 °C

With hydrogen bromide; potassium carbonate; silver carbonate; silver(l) oxide; In methanol; dichloromethane; toluene;