methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate

Base Information

Chemical Name:methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate
CAS No.:741716-51-8
Molecular Formula:C₁₉H₁₆N₂O₇
Molecular Weight:384.345
Hs Code.:

Synonyms:methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate

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Chemical Property of methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate

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Technology Process of methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate

There total 2 articles about methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 114106-93-3
methyl 2-[hydroxy(4-nitrophenyl)methyl]prop-2-enoate

: 4461-33-0
benzoyl isocyanate

: 741716-51-8
methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate

Guidance literature:: In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ol049146j

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 741716-51-8
methyl 3-benzoylaminocarbonyloxy-2-methylene-3-(4-nitrophenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DABCO / 360 h / 20 °C

2: 100 percent / CH₂Cl₂ / 3 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; 1: Baylis-Hillman reaction;
DOI:10.1021/ol049146j