ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

Base Information

Chemical Name:ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate
CAS No.:1097223-25-0
Molecular Formula:C₂₄H₂₀Cl₃N₃O₃
Molecular Weight:504.8
Hs Code.:

Synonyms:ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

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Chemical Property of ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

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Technology Process of ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

There total 3 articles about ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 121641-61-0
(4-chloro-phenylimino)-acetic acid ethyl ester

: 78-94-4,25038-87-3
methyl vinyl ketone

: 22289-05-0
3-methyleneheptane-2,6-dione

: 1097223-25-0
ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

Guidance literature:: With diphenyl(methyl)phosphine; In acetonitrile; at 20 ℃; for 48h; Molecular sieve; Inert atmosphere;
DOI:10.1039/b811167g

Reference yield:

: 121641-61-0
(4-chloro-phenylimino)-acetic acid ethyl ester

: 1097223-25-0
ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

Guidance literature:: With potassium fluoride; 18-crown-6 ether; In acetonitrile; at 25 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.orglett.6b02186

Reference yield:

: 106-47-8
4-chloro-aniline

: 1097223-25-0
ethyl 1,3-bis(4-chlorophenyl)-4-((4-chlorophenyl)amino)-5-oxoimidazolidine-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate / toluene / 1 h / 25 °C / Inert atmosphere

2: potassium fluoride; 18-crown-6 ether / acetonitrile / 2 h / 25 °C / Inert atmosphere; Molecular sieve

With potassium fluoride; 18-crown-6 ether; magnesium sulfate; In toluene; acetonitrile;
DOI:10.1021/acs.orglett.6b02186