2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone

Base Information

• Chemical Name: 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone
• CAS No.: 70602-99-2
• Molecular Formula: C₃₂H₃₇N₃O₂
• Molecular Weight: 495.665

Synonyms:2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone

Chemical Property of 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone

Chemical Property:

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Technology Process of 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone

There total 2 articles about 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 6-morpholino-3,4-dihydro-1(2H)-naphthalenone hydrochloride (70602-98-1) + 1-benzhydrylpiperazine hydrochloride (56609-03-1) → 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone (70602-99-2)

Guidance literature:

With sodium bicarbonate; In ethanol;

Reference yield:

6-morpholino-3,4-dihydro-1(2H)-naphthalenone (15300-12-6) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-benzhydrylpiperazine hydrochloride (56609-03-1,57311-01-0,66090-75-3) → 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone (70602-99-2)

Guidance literature:

In ethanol; Ambient temperature;

DOI:10.1248/cpb.31.2006

Reference yield:

2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-3,4-dihydro-1(2H)-naphthalenone (70602-99-2) → 2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-1,2,3,4-tetrahydro-1-naphthalenol (70603-00-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; chloroform; for 0.5h; Ambient temperature;

DOI:10.1248/cpb.31.2006

upstream raw materials:

6-morpholino-3,4-dihydro-1(2H)-naphthalenone

formaldehyd

N-benzhydrylpiperazine hydrochloride

6-morpholino-3,4-dihydro-1(2H)-naphthalenone hydrochloride

Downstream raw materials:

2-[(4-benzhydryl-1-piperazinyl)methyl]-6-morpholino-1,2,3,4-tetrahydro-1-naphthalenol

(1S,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-6-morpholin-4-yl-1,2,3,4-tetrahydro-naphthalen-1-ol

(1R,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-6-morpholin-4-yl-1,2,3,4-tetrahydro-naphthalen-1-ol

(1S,2S)-2-(4-Benzhydryl-piperazin-1-ylmethyl)-6-morpholin-4-yl-1,2,3,4-tetrahydro-naphthalen-1-ol; compound with (E)-but-2-enedioic acid

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