Technology Process of C13H14O4S
There total 6 articles about C13H14O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert.-butylhydroperoxide; molybdenum hexacarbonyl;
In
decane; benzene;
at 85 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c0cc05405d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10 h / 0 - 20 °C / Inert atmosphere
2: tert.-butylhydroperoxide; molybdenum hexacarbonyl / decane; benzene / 1 h / 85 °C / Inert atmosphere
With
tert.-butylhydroperoxide; 3-chloro-benzenecarboperoxoic acid; molybdenum hexacarbonyl;
In
decane; dichloromethane; benzene;
DOI:10.1039/c0cc05405d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
1.2: 6 h / 20 °C / Inert atmosphere
2.1: trimethylsilyl trifluoromethanesulfonate; triethylamine / dichloromethane / 8 h / Inert atmosphere; Reflux
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10 h / 0 - 20 °C / Inert atmosphere
4.1: tert.-butylhydroperoxide; molybdenum hexacarbonyl / decane; benzene / 1 h / 85 °C / Inert atmosphere
With
tert.-butylhydroperoxide; trimethylsilyl trifluoromethanesulfonate; sodium hexamethyldisilazane; triethylamine; 3-chloro-benzenecarboperoxoic acid; molybdenum hexacarbonyl;
In
tetrahydrofuran; decane; dichloromethane; benzene;
DOI:10.1039/c0cc05405d
