6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

Base Information

Chemical Name:6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose
CAS No.:1263312-79-3
Molecular Formula:C₇₀H₇₅IO₁₀Si
Molecular Weight:1231.35
Hs Code.:

Synonyms:6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

Suppliers and Price of 6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

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Technology Process of 6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

There total 2 articles about 6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1033507-59-3
1',2,3,3',4,4'-hexa-O-benzyl-6'-O-(tert-butyldiphenylsilyl)-6-O-(methylsulfonyl)sucrose

: 1263312-79-3
6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 120 ℃; for 72h;
DOI:10.1080/07328303.2010.524958

Reference yield:

: 900525-72-6
6’-O-tert-butyldiphenylsilyl-1’,2,3,3’,4,4’-hexa-O-benzylsucrose

: 1263312-79-3
6-iodo-6-deoxy-6'-(tert-butyldiphenylsilyl)-1',2,3,3',4,4'-hexa-O-benzylsucrose

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 16 h / 20 °C

2: potassium iodide / N,N-dimethyl-formamide / 72 h / 120 °C

With dmap; triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328303.2010.524958