C₄₃H₅₆O₉Si

Base Information

Chemical Name:C₄₃H₅₆O₉Si
CAS No.:162088-47-3
Molecular Formula:C₄₃H₅₆O₉Si
Molecular Weight:744.998
Hs Code.:

C<sub>43</sub>H<sub>56</sub>O<sub>9</sub>Si

Synonyms:C₄₃H₅₆O₉Si

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Chemical Property of C₄₃H₅₆O₉Si

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Technology Process of C₄₃H₅₆O₉Si

There total 9 articles about C₄₃H₅₆O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 162088-46-2
C₄₁H₅₄O₈Si

: 162088-47-3
C₄₃H₅₆O₉Si

Guidance literature:: With dmap; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1021/ja00107a009

Reference yield:

: 994-30-9
triethylsilyl chloride

: 162088-47-3
C₄₃H₅₆O₉Si

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / dimethylformamide / 1 h / 25 °C

2: DMAP / CH₂Cl₂ / 0.5 h / 25 °C

With dmap; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00107a009

Reference yield:

: 162088-38-2
C₃₀H₃₆O₉

: 162088-47-3
C₄₃H₅₆O₉Si

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu₄NBH₄

2: 76 percent / KH, n-Bu₄NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C

3: 98 percent / DBU / methanol; CH₂Cl₂ / 3 h / 25 °C

4: DMAP / dimethylformamide / 1 h / 25 °C

5: DMAP / CH₂Cl₂ / 0.5 h / 25 °C

With dmap; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00107a009