ethylphenylphosphine-borane

Base Information

Chemical Name:ethylphenylphosphine-borane
CAS No.:568600-64-6
Molecular Formula:C₈H₁₄BP
Molecular Weight:151.984
Hs Code.:

Synonyms:ethylphenylphosphine-borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethylphenylphosphine-borane

Chemical Property:

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Technology Process of ethylphenylphosphine-borane

There total 7 articles about ethylphenylphosphine-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: C₁₂H₂₃BNP

: 568600-64-6
ethylphenylphosphine-borane

: C₁₂H₂₅BNP

Guidance literature:: C₁₂H₂₃BNP; With ammonia; sodium; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique; Cooling with acetone-dry ice;

With ammonium chloride; In tetrahydrofuran; Inert atmosphere; Schlenk technique; Cooling with acetone-dry ice;
DOI:10.1002/ejoc.201800065

Reference yield:

: 3619-88-3
ethylphenylphosphine

: 568600-64-6
ethylphenylphosphine-borane

Guidance literature:: With borane-THF; In toluene; at 0 - 20 ℃;
DOI:10.1039/b920324a

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 568600-64-6
ethylphenylphosphine-borane

Guidance literature:: Multi-step reaction with 5 steps

1: 1-methyl-1H-imidazole / methyl cyclohexane / 1 h / 20 °C

2: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: hydrogenchloride; water / diethyl ether / 0 °C

4: titanium(IV) isopropylate; 1,1,3,3-Tetramethyldisiloxane / toluene / 60 °C / Inert atmosphere

5: borane-THF / toluene / 0 - 20 °C

With 1-methyl-1H-imidazole; titanium(IV) isopropylate; hydrogenchloride; borane-THF; 1,1,3,3-Tetramethyldisiloxane; water; In tetrahydrofuran; diethyl ether; methyl cyclohexane; toluene;
DOI:10.1039/b920324a