(3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide

Base Information

• Chemical Name: (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide
• CAS No.: 323195-88-6
• Molecular Formula: C₁₃H₁₉IO₂
• Molecular Weight: 334.197
• Mol file: 323195-88-6.mol

Synonyms:(3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide

Chemical Property of (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide

There total 5 articles about (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Toluene-4-sulfonic acid (S)-3-(2,5-dimethoxy-4-methyl-phenyl)-butyl ester → (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide (323195-88-6)

Guidance literature:

With sodium iodide; In acetone; for 2h; Heating;

DOI:10.1039/b006141g

Reference yield:

(2E)-3-(2,5-Dimethoxy-4-methylphenyl)but-2-enal (323195-92-2) → (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide (323195-88-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 56 percent / resin XAD 1180; fermenting baker's yeast; aq. glucose / 132 h / 20 °C

2: pyridine / CH₂Cl₂ / 5 h / 20 °C

3: NaI / acetone / 2 h / Heating

With pyridine; D-glucose; fermenting Baker's Yeast; resin XAD 1180; sodium iodide; In dichloromethane; acetone;

DOI:10.1039/b006141g

Reference yield:

(3S)-3-(2,5-Dimethoxy-4-methylphenyl)butan-2-ol (323195-93-3) → (3S)-3-(2,5-Dimethoxy-4-methylphenyl)butyl iodide (323195-88-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 5 h / 20 °C

2: NaI / acetone / 2 h / Heating

With pyridine; sodium iodide; In dichloromethane; acetone;

DOI:10.1039/b006141g

upstream raw materials:

(2E)-3-(2,5-Dimethoxy-4-methylphenyl)but-2-enal

3-(2,5-dimethoxy-4-methylphenyl)but-2-enol

(3S)-3-(2,5-Dimethoxy-4-methylphenyl)butan-2-ol

Ethyl (2E)-3-(2,5-dimethoxy-4-methylphenyl)but-2-enoate

Downstream raw materials:

(S)-(-)-Curcuquinone

(S)-(+)-Curcuhydroquinone

(S)-1-(2,5-dimethoxy-4-methylphenyl)ethyl diisopropylcarbamate