dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

Base Information

Chemical Name:dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate
CAS No.:1269247-09-7
Molecular Formula:C₃₃H₂₈O₅
Molecular Weight:504.582
Hs Code.:

Synonyms:dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

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Technology Process of dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

There total 1 articles about dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 624-31-7
4-tolyl iodide

: 1236300-95-0
dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(prop-2-ynyl)malonate

: 1269247-09-7
dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol102920f

Reference yield: 86.0%

: 201230-82-2
carbon monoxide

: 1269247-09-7
dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

: 1262638-30-1
C₃₄H₂₈O₆

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; In 1,2-dichloro-ethane; at 60 ℃; for 8h; under 760.051 Torr;
DOI:10.1021/ol102920f

Reference yield: 72.0%

: 603-76-9
1-methylindole

: 1269247-09-7
dimethyl 2-(4-benzoyl-5-phenylpent-4-en-2-ynyl)-2-(3-p-tolylprop-2-ynyl)malonate

: 1269247-33-7
C₄₂H₃₅NO₅

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); lithium bromide monohydrate; In acetonitrile; at 40 ℃; for 26h;
DOI:10.1002/adsc.201000670