C₂₄H₃₃ClO₄

Base Information

Chemical Name:C₂₄H₃₃ClO₄
CAS No.:916323-71-2
Molecular Formula:C₂₄H₃₃ClO₄
Molecular Weight:420.977
Hs Code.:

C<sub>24</sub>H<sub>33</sub>ClO<sub>4</sub>

Synonyms:C₂₄H₃₃ClO₄

Suppliers and Price of C₂₄H₃₃ClO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₃₃ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₃₃ClO₄

There total 14 articles about C₂₄H₃₃ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C₂₄H₃₇ClO₄: C₂₄H₃₇ClO₄

: 916323-71-2
C₂₄H₃₃ClO₄

Guidance literature:: C₂₄H₃₇ClO₄; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1039/c2ob25100k

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 916323-71-2
C₂₄H₃₃ClO₄

Guidance literature:: Multi-step reaction with 13 steps

1.1: piperidine / 5,5-dimethyl-1,3-cyclohexadiene / 0.5 h / 160 °C / Inert atmosphere

1.2: 3.5 h / 155 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

4.2: 17 h / -78 - -20 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

6.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

6.2: 5 h / 0 - 20 °C / Inert atmosphere

7.1: sodium periodate / methanol / 0.5 h / 20 °C / pH 7 / aq. buffer; Inert atmosphere

8.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

8.2: 46 h / -78 - -20 °C / Inert atmosphere

9.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

10.1: (triphenylphosphine)copper(I) hydride hexamer; phenylsilane / toluene / 0.5 h / 0 - 20 °C / Inert atmosphere

11.1: diisobutylaluminium hydride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

12.1: hydrogenchloride / water; acetonitrile / 2 h / 20 °C / Inert atmosphere

13.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

13.2: 2.5 h / -78 - 0 °C / Inert atmosphere

With piperidine; 2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; (triphenylphosphine)copper(I) hydride hexamer; phenylsilane; dicyclohexylboron chloride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; dichloromethane; water; toluene; acetonitrile; 1.1: Knoevenagel reaction / 1.2: Knoevenagel reaction / 3.1: Dess-Martin oxidation / 4.1: Aldol condensation / 4.2: Aldol condensation / 8.1: Aldol condensation / 8.2: Aldol condensation / 13.1: Swern oxidation / 13.2: Swern oxidation;
DOI:10.1039/c2ob25100k

Reference yield:

: 916323-73-4
(E)-6-Benzyloxy-hex-3-enal

: 916323-71-2
C₂₄H₃₃ClO₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

1.2: 17 h / -78 - -20 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

3.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

3.2: 5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium periodate / methanol / 0.5 h / 20 °C / pH 7 / aq. buffer; Inert atmosphere

5.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 1 h / -78 - 0 °C / Inert atmosphere

5.2: 46 h / -78 - -20 °C / Inert atmosphere

6.1: methanesulfonyl chloride; triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

7.1: (triphenylphosphine)copper(I) hydride hexamer; phenylsilane / toluene / 0.5 h / 0 - 20 °C / Inert atmosphere

8.1: diisobutylaluminium hydride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

9.1: hydrogenchloride / water; acetonitrile / 2 h / 20 °C / Inert atmosphere

10.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

10.2: 2.5 h / -78 - 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; oxalyl dichloride; (triphenylphosphine)copper(I) hydride hexamer; phenylsilane; dicyclohexylboron chloride; diisobutylaluminium hydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; In methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile; 1.1: Aldol condensation / 1.2: Aldol condensation / 5.1: Aldol condensation / 5.2: Aldol condensation / 10.1: Swern oxidation / 10.2: Swern oxidation;
DOI:10.1039/c2ob25100k