((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane

Base Information

• Chemical Name: ((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane
• CAS No.: 1039740-36-7
• Molecular Formula: C₃₄H₅₂O₇Si
• Molecular Weight: 600.868

Synonyms:((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane

Chemical Property of ((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane

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Technology Process of ((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane

There total 1 articles about ((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(1S,2R,3S,4S,6R)-4-(tert-butyldimethylsilyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-1-ol (1039740-34-5) + benzyl bromide (100-39-0) → ((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane (1039740-36-7)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1021/jo800913x

Reference yield: 95.0%

((1S,2R,3S,4S,6R)-1-(benzyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-4-yloxy)(tert-butyl)dimethylsilane (1039740-36-7) → ((1S,2R,3S,4S,6R)-1-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-3-(2,2-dimethoxyethyl)-3-methyl-7-oxabicyclo[4.2.0]octan-2-yl)methanol (1039740-38-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 0 ℃; for 1h;

DOI:10.1021/jo800913x

upstream raw materials:

(1S,2R,3S,4S,6R)-4-(tert-butyldimethylsilyloxy)-3-(2,2-dimethoxyethyl)-2-((4-methoxybenzyloxy)methyl)-3-methyl-7-oxabicyclo[4.2.0]octan-1-ol

benzyl bromide

Downstream raw materials:

((1S,2R,3S,4S,6R)-1-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-3-(2,2-dimethoxyethyl)-3-methyl-7-oxabicyclo[4.2.0]octan-2-yl)methanol

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